Related Products of 79574-70-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 79574-70-2, name is 3-Acetyl-2-fluoropyridine, molecular formula is C7H6FNO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Step 2: 3-methyl-lH-pyrazolo[3,4-b]pyridine (36-2); A stirred solution of 1.1 Og (7.91 mmol) of l-(2-fluoropyridine-3-yl)ethanone in 5 mL of ethylene glycol under nitrogen was treated with 265 muL (8.31 mmol) of hydrazine. This solution was stirred for 2 hours at room temperature and then heated at 165C for 1.5 hours. The solution was cooled to room temperature, poured into CH2CI2 (25 mL), and extracted with H2O (2×50 mL). The organic portions were combined, dried (MgSO-O, filtered and concentrated in vacuo to give the title product as a fluffy off-white solid. lH NMR (CDCI3): delta 2.6 l(s, 3H), 7.14(m,lH), 8.06(dd,lH), 8.58(dd,lH), 11.18(br s, IH).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 79574-70-2, 3-Acetyl-2-fluoropyridine.
Reference:
Patent; MERCK & CO., INC.; WO2008/76223; (2008); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem