14/9/2021 News A new synthetic route of 6231-18-1

At the same time, in my other blogs, there are other synthetic methods of this type of compound,6231-18-1, 2,6-Dimethoxypyridine, and friends who are interested can also refer to it.

With the rapid development and complex challenges of chemical substances, the synthesis of new drugs is usually one of the most effective ways to increase yield.6231-18-1, name is 2,6-Dimethoxypyridine, molecular formula is C7H9NO2, molecular weight is 139.15, as common compound, the synthetic route is as follows.Application In Synthesis of 2,6-Dimethoxypyridine

Comparative Example 1 In a 50 cc short-neck flask, 0.751 g of 2,6-dimethoxypyridine, 18 ml of 35% hydrochloric acid and 18 ml of acetic acid were placed, and then the flask was dipped in an oil bath of 140 C. while conducting stirring reflux for 1 hour. The reaction mixture was analyzed using liquid chromatography, showing a yield of 2,6-dihydroxypyridine of 28.8% and a residual ratio of the starting material (2,6-dimethoxypyridine) of 51.2%.

At the same time, in my other blogs, there are other synthetic methods of this type of compound,6231-18-1, 2,6-Dimethoxypyridine, and friends who are interested can also refer to it.

Reference:
Patent; Kato, Syunsaku; Suzuki, Daisuke; Seo, Yoshiko; US2002/157939; (2002); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem