16-Sep-21 News The origin of a common compound about 15471-17-7

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,15471-17-7, its application will become more common.

Adding a certain compound to certain chemical reactions, such as: 15471-17-7, 3-(Pyridin-1-ium-1-yl)propane-1-sulfonate, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 15471-17-7, blongs to pyridine-derivatives compound. HPLC of Formula: C8H11NO3S

General procedure: Toa mixture of toluene (30 mL) and 1,3-propane sulfone (0.10 mol, 12.2 g) in a 100 mLround bottomed flask was added pyridine (0.11 mol, 8.7 g, 8.9 mL). The reactionmixture was stirred for 24 h at 50 oC under a nitrogen atmosphereuntil a white precipitate (PyPS) was formed. After filtration, washing withdiethyl ether and drying in a vacuum, PyPS was obtained. To an aqueous solutionof H3PW12O40 (0.03 mol, 86.4 g) was added PyPS(0.09 mol, 18.1 g) and then the mixture was stirred at room temperature for 24h. Finally, the solution was removed in vacuum to give the product [PyPS]3PW12O40as a solid. Thus [MIMPS]3PW12O40, [MIMPS]3PMo12O40,[PyPS]3PMo12O40, [TEAPS]3PW12O40and [TEAPS]3PMo12O40 were prepared usingaccording starting materials.

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,15471-17-7, its application will become more common.

Reference:
Article; Fu, Renzhong; Yang, Yang; Ma, Yunsheng; Yang, Fei; Li, Jingjing; Chai, Wen; Wang, Quan; Yuan, Rongxin; Tetrahedron Letters; vol. 56; 30; (2015); p. 4527 – 4531;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem