Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1195-59-1, name is 2,6-Pyridinedimethanol. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 1195-59-1
At 0 C, a solution of p-toluenesulfonyl chloride (0.76 g,4.0 mmol) in tetrahydrofuran (THF; 7.5 mL) was added to a stirred solution of 2,6-pyridinedimethanol (0.28 g, 2.0 mmol) and NaOH (0.8 g, 20 mmol) in THF/water (7.5/7.5 mL). After 4 h of stirring, the mixture was poured into 20 mL of water and extracted with methylene chloride (3 × 7.5 mL). The organic phase was washed with saturated aqueous NaCl solution and distilled water and dried over Na2SO4; the solvent was removed in vacuo to afford 2,6-pyridinedimethylene ditosylate (0.79 g, 88%) as a white powder. 1H NMR(300 MHz, CDCl3): = 7.80 (d, J = 7.5 Hz, 4H, 2,6-H tosyl), 7.69 (t,J = 7.5 Hz, 1H, 4-H Py), 7.32 (d, 2H, 3,5-H Py, d, 4H, 3,5-H tosyl), 5.04(s, 4H, PyCH2tosyl), and 2.44 (s, 6H, tosyl-CH3)
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Reference:
Article; Woo, Jeong Oh; Kang, Sung Kwon; Park, Jong-Eun; Son, Kyung-Sun; Journal of Molecular Catalysis A: Chemical; vol. 404-405; (2015); p. 204 – 210;,
Pyridine – Wikipedia,
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