Application of 1124-64-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 1124-64-7, name is 1-Butylpyridinium Chloride. This compound has unique chemical properties. The synthetic route is as follows.
1Butylpyridinium chloride [BPy][Cl] (0.2580 g, 1.46 mmol) wasdissolved in 15 mL of methanol and to this solution the ionexchange resin Amberlyst A26 (OH-) (9.13 mL, 7.3 mmol) wasadded and it was kept in stirring for 1 h in order to exchange thechloride to the hydroxide form. The resin was filtered and washedwith methanol. To the resultant filtrate, H3PMo12O40 (0.973 g,0.53 mmol) in methanol was slowly added, a yellow precipitateimmediately formed and the mixture was stirred at room temperaturefor 1 h. The product was filtered, washed several times withmethanol and dried in the oven at 80 C overnight (1.05 g, 89%). 1H NMR (400.13 MHz, DMSO d6, 25C) delta = 9.10 (d, J = 4.0 Hz,2H), 8.63 (t, J = 8.0 Hz, 1H), 8.19 (t, J = 8.0 Hz, 2H), 4.63(t, J = 8.0 Hz, 2H), 1.95 (m, J = 8.0 Hz, 2H), 1.31 (m, 2H), 0.94(t, J = 8.0 Hz, 3H) ppm. 31P NMR (162 MHz, CD3CN, 25 C)delta = -2.09 ppm. Selected FTIR (cm-1, KBr): 3124 (w), 3080 (w),3063 (w), 2963 (w), 2929 (w), 2869 (w), 1632 (s), 1581(w), 1485 (s), 1462 (m), 1384 (w), 1316 (w), 1278 (w), 1209 (w),1168 (m), 1063 (vs), 956 (vs), 878 (s), 795 (s), 682 (s), 644 (w),594 (w), 504 (m). Anal. Calc. for (C9H14N)3PMo12O40 (2230.87): C,15.04; H, 1.88; N, 1.87; Found: C, 14.76; H, 1.85; N, 1.87
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 1124-64-7, 1-Butylpyridinium Chloride.
Reference:
Article; Mirante, Fatima; Gomes, Neide; Corvo, Marta C.; Gago, Sandra; Balula, Salete S.; Polyhedron; vol. 170; (2019); p. 762 – 770;,
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