Electric Literature of 5470-70-2, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 5470-70-2, name is Methyl 6-methylnicotinate. This compound has unique chemical properties. The synthetic route is as follows.
Production Example 1-1: Methyl 6-bromomethylnicotinate To a solution of methyl 6-methylnicotinate (50g, 331mmol) in carbon tetrachloride (625mL), was added N-bromosuccinimide (59g, 331mmol). Further 1.0g of benzoyl peroxide was added, the mixture was reacted at a temperature from 40 to 50C for 24 hours with irradiation of light from a projector. After the reaction mixture was cooled, the precipitated crystals were separated by filtration. The filtrate was washed with an aqueous solution containing sodium hydrogencarbonate, and concentrated. The residue obtained by the concentration was purified by silica gel column chromatography, thereby to yield 37g of the target compound. 1H-NMR (CDCl3, 300MHz): delta 3.96(3H, s, OCH3), 4.58(2H, s, CH2Br), 7.54(1H, d, Py), 8.30(1H, dd, Py), 9.17(1H, d, Py)
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 5470-70-2, Methyl 6-methylnicotinate.
Reference:
Patent; KABUSHIKI KAISHA NARD KENKYUSHO; EP1455189; (2004); A1;,
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