9/18/21 News Extracurricular laboratory: Synthetic route of 15471-17-7

According to the analysis of related databases, 15471-17-7, the application of this compound in the production field has become more and more popular.

Related Products of 15471-17-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 15471-17-7, name is 3-(Pyridin-1-ium-1-yl)propane-1-sulfonate. This compound has unique chemical properties. The synthetic route is as follows.

Please refer to FIG. 2 and FIG. 3, which are a view showing reactions of fabricating the IL; and a view showing transacylation and stratification. As shown in the figures, on using the present invention, for fabricating an acidic IL as a catalyst, pyridine or 1-butyl-imidazole (N-butyl imidazole) is reacted with 1,3-propane sultone at 40 C. for 24 hrs to obtain a white solid of a zwitterionic compound. After being purified with ether and dried through vacuuming, the white solid of the zwitterionic compound of R+-(CH2)3-SO3- is obtained, where R is pyridine or 1-butyl-imidazole (i.e. n-propane sulfonic acid pyridinium (PSPy) or pyridinium propyl sulfobetaine (PPS)). An appropriate amount of the white solid is obtained in a round bottom flask to be added with a considerable number of moles of sulfuric acid for reaction with stirring at 100 C. for 0.5 hr. A transparent viscous liquid is gradually formed, which is an acidic IL of [R+-(CH2)3-SO3H][HSO4] obtained through the reaction shown in FIG. 2.

According to the analysis of related databases, 15471-17-7, the application of this compound in the production field has become more and more popular.

Reference:
Patent; CPC CORPORATION, TAIWAN; Wu, Jung-Chung; Huang, Ming-Yu; Lin, Jann-Chen; Wang, Yih-Ping; (11 pag.)US9586886; (2017); B1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem