Reference of 65873-72-5, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 65873-72-5, name is 6-Methoxynicotinaldehyde, molecular formula is C7H7NO2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
A stirred solution of 6-methoxy-3-pyridmecarboxaldehyde (0.45g, 3.3mMol) in 3N HCl(1OmL) was heated to 1000C for 30 minutes. Upon cooling, needle-like crystals developed. The crystals were collected via filtration to yield 17-2. 1H-NMR (CD3OD) delta 9.64 (s, IH), delta 8.17-8.16 (m, IH), delta 7.96-7.94 (m, IH), delta 6.58(d, IH).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 65873-72-5, 6-Methoxynicotinaldehyde.
Reference:
Patent; MERCK & CO., INC.; WO2006/135627; (2006); A2;,
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