Reference of 1132-37-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 1132-37-2, name is Dipyridin-2-ylmethane, molecular formula is C11H10N2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
100cc Schlenk tube and then in the oxygen and three times replacement with argon and vacuum for removal of water Pt[2,2′-bpyridine]Cl2 (90.34mg, 0.214mmol) was added and dissolved with EtOH solvent (20ml). To this solution was added dipyridin-2-ylmethane (40mg, 0.235mmol) was dissolved in EtOH (15ml). The mixture is contained in a Schlenk tube for 5 hours and then put Reflux NH4PF6 (114.9mg, 0.705mmol) was refluxed with 80C for 36 hours under argon gas. After confirming the completion of the reaction by TLC whether the mixture was cooled at room temperature. Conducted a filter to remove the resulting precipitate was cooled, and the supernatant was filtered through a filter and then dried in vacuum and then washed CHCl3 to give the title compound (yield: 57%).
According to the analysis of related databases, 1132-37-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Sunchon National University Industry-Academic Cooperation Foundation; Jung, Min Chul; Kim, Song Chan; (13 pag.)KR101602456; (2016); B1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem