The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 6515-09-9, name is 2,3,6-Trichloropyridine. This compound has unique chemical properties. The synthetic route is as follows. HPLC of Formula: C5H2Cl3N
A mixture of 2,3,6-trichloropyridine (18.2 g, 0.1 mol)Pd / C (10%) (2.73 g),1-isopropyl-4-methylcyclohexene (69 g, 0.5 mol) was added to methanol (182 g)Slowly heated to 60 C for 4 hours;After the reaction,The methanol was distilled off by distillation and vacuum distillation,Add water (100 g),The mixture of 2,3-dichloropyridine and water was distilled off by steam distillation at atmospheric pressure,Cooled by filtration to obtain 2,3-dichloropyridine 14g,Purity (HPLC) ?98%Yield 95%.
With the rapid development of chemical substances, we look forward to future research findings about 6515-09-9.
Reference:
Patent; Jiangsu Zhongbang Pharmaceutical Co., Ltd.; Qian, Yong; Xu, Qiang; Gao, Qian; Zhao, Huayang; Zhang, Xiaoqing; (5 pag.)CN106518754; (2017); A;,
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