Adding a certain compound to certain chemical reactions, such as: 1137-67-3, 2-(Pyridin-3-yl)-1H-benzo[d]imidazole, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Product Details of 1137-67-3, blongs to pyridine-derivatives compound. Product Details of 1137-67-3
A reaction mixture of CdI2 (73.2 mg, 0.2 mmol), 3-PyBim (19.5 mg, 0.1 mmol), and water(10 ml) was added to a 15 ml Teon reactor under autogenous pressure at 160 C for 3 days and then cooled to room temperature at 5 C h-1. Pale yellow crystals of 1 suitable for diffraction analysis were obtained. (31 mg, Yield: 25.2%). Analysis found (%): C, 48.89; H, 3.50;N, 13.95; requires (%): C, 48.00; H, 3.52; N, 13.99; IR (KBr, cm-1): 3493 (m), 3169 (w), 3051 (w),3010 (w), 2993 (w), 2929 (w), 2887 (w), 2794 (w), 2717 (w), 2603 (w), 2189 (w), 1581 (m), 1483(m), 1433 (s), 1317 (m), 1280 (m), 1226 (m), 1192 (m), 1120 (m), 1047 (m), 966 (m), 923 (w),817 (m), 744 (s), 700 (m), 638 (m), 408 (w).
The synthetic route of 1137-67-3 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Wang, Jin-Hua; Tang, Gui-Mei; Qin, Ting-Xiao; Wang, Yong-Tao; Cui, Yue-Zhi; Ng, Seik Weng; Journal of Coordination Chemistry; vol. 70; 7; (2017); p. 1168 – 1189;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem