Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 573762-62-6, name is 5-Amino-3-(trifluoromethyl)picolinonitrile. This compound has unique chemical properties. The synthetic route is as follows. name: 5-Amino-3-(trifluoromethyl)picolinonitrile
To a heterogeneous mixture of 2-cyano-3- (trifluoromethyl)-5-nitropyridine, A 11 (0.075 g, 0.4 mmol) in water (2 ml), thiophosgene (50 mu l) wasadded. This mixture was stirred for 2 hours, then washed with water, andextracted with chloroform. The organic layer was dried over MgSO4,concentrated to give a compound A12 (0.087g, 0.38mmol, 95%).
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Reference:
Patent; THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; JUNG, MICHAEL E; SAWYERS, CHARLES L; OUK, SAMEDY; TRAN, CHRIS; WONGVIPAT, JOHN; (40 pag.)JP2016/11315; (2016); A;,
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