Electric Literature of 54221-96-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 54221-96-4, name is 6-Methoxypicolinaldehyde, molecular formula is C7H7NO2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
General procedure: General procedure: 8-Hydrazinocaffeine (3) (112 mg;0.5 mmol) and carbonyl compound (1 mmol; 2 eq.) were mixedin ethanol (20 mL, containing 0.2 mL of acetic acid) and heated at 75 omicronC for 3 days. After cooling down, reaction mixture was evaporatedto dryness and solid residue was suspended in diethyl ether(50 mL), filtered off, washed with additional portion of diethylether (3 25 mL) and dried in vacuo at 50 C to obtain the hydrazone.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 54221-96-4, 6-Methoxypicolinaldehyde.
Reference:
Article; Kaplanek, Robert; Jakubek, Milan; Rak, Jakub; Kejik, Zden?k; Havlik, Martin; Dolensky, Bohumil; Frydrych, Ivo; Hajduch, Marian; Kola?, Milan; Bogdanova, Kate?ina; Kralova, Jarmila; D?ubak, Petr; Kral, Vladimir; Bioorganic Chemistry; vol. 60; (2015); p. 19 – 29;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem