Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 5349-17-7, name is 2-Bromo-1-(pyridin-4-yl)ethanone hydrobromide. This compound has unique chemical properties. The synthetic route is as follows. name: 2-Bromo-1-(pyridin-4-yl)ethanone hydrobromide
A solution of 4-(bromoacetyl)pyridine hydrobrornide (2 g, 7. 12 mmol) andthiobenzamide (976 mg, 7.12 rnmol) in absolute EtOH (20 mL) was stirred at 80 C)C for l.Sh,cooled to room temperature, and concentrated in vacuo. The resulting solid was trinLrated withsaturated aqueous potassium carbonate, filtered, washed with water, and dried in vacuo to give1.57 g of the title product as a light pink solid (92% yield): 1 H Ntv1R (DMSO-d6. ppm) o 7.58(m, 3H), 8.03 (d, 2H), 8.08 (dd, 2H), 8.56 (s, l H), 8.70 (d, 2H); [M+H ‘J rn/z 239.
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Reference:
Patent; RUGA CORPORATION; VERNIER, Jean-Michel; O’CONNOR, Patrick; BOUNAUD, Pierre-Yves; HOPKINS, Stephanie; MATTHEWS, David; WO2014/172639; (2014); A1;,
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