Related Products of 6295-87-0, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 6295-87-0, name is 1-Aminopyridinium Iodide. This compound has unique chemical properties. The synthetic route is as follows.
But-3-yn-2-one (0.71g, 10.4mmol) and 1-aminopyridinium iodide (2.69g, 12mmol) were dissolved in DMSO (21mL) and treated with K2CO3 (1.30g, 9.36mmol) and KOH (1.17g, 20.8mmol). The mixture was stirred for 6hat room temperature. Then the reaction mixture was poured in water (50mL) and extracted with ethyl acetate (15mL¡Á3), the combined organic phase was washed with brine (20mL¡Á2), dried over anhydrous Na2SO4 and concentrated. The residue was purified by column chromatography (eluent: petroleum ether/ethyl acetate=4:1) to provide 12o as a pale yellow solid (0.53g, 31%). Mp: 94-96C (Lit.Mp [19]: 102-103C). 1H NMR (400MHz, CDCl3): delta=2.56 (s, 3H), 7.01 (t, J=8.0Hz, 1H), 7.47 (t, J=8.0Hz, 1H), 8.34-8.40 (m, 2H), 8.54 (d, J=8.0Hz, 1H).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 6295-87-0, 1-Aminopyridinium Iodide.
Reference:
Article; Li, Ri-Dong; Wang, Hui-Ling; Li, Ying-Bo; Wang, Zhong-Qing; Wang, Xin; Wang, Yi-Tao; Ge, Ze-Mei; Li, Run-Tao; European Journal of Medicinal Chemistry; vol. 93; (2015); p. 381 – 391;,
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