As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 694-85-9, name is 1-Methylpyridin-2(1H)-one, molecular formula is C6H7NO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. HPLC of Formula: C6H7NO
0.8mmol), compound A-3 (0.4mmol, 1 eq.), Three times with nitrogen was added 3mLpermuted dimethylsulfoxide (DMSO), injection of 100muL (0.80mmol) Compound B-1, wasstirred for 24 hours under blue light , compound C-3. The yield was 60percent.
With the rapid development of chemical substances, we look forward to future research findings about 694-85-9.
Reference:
Patent; Zunyi Medical College; He, Chunyang; Li, Xiaofei; (12 pag.)CN105669546; (2016); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem