Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 91-02-1, name is Phenyl(pyridin-2-yl)methanone. This compound has unique chemical properties. The synthetic route is as follows. Safety of Phenyl(pyridin-2-yl)methanone
Phenylpyridinone (36.5mg, 0.2mmol), dichlorantin (39.4mg, 0.2mmol) and Pd (OAc) 2 (4.5mg, 0.02mmol),2mL of dichloroethane was added, and the reaction was carried out at 90 C for 12h. Purified by thin-layer chromatography to obtain 21.7mg of 2-chlorophenylpyridylmethanone with a yield of 50.0%.
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Reference:
Patent; China Three Gorges University; Liu Qixing; Chen Yongsheng; Zhang Yin; Chen Danyi; Wen Simiaomiao; Zhao Rongrong; Liu Yiheng; Zhou Haifeng; (14 pag.)CN110563641; (2019); A;,
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