Application of 1609373-99-0, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 1609373-99-0, name is 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine, molecular formula is C17H12N2O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Intermediate I-3 (3.9 g, 5.2 mmol) and ligand L-2 (3.8 g, 15.6 mmol)Dissolved in DMF (100 mL) and 2-ethoxyethanol (100 mL)The mixture was heated at 130 C for 18 hours.After evaporating the solvent, the crude product contains 65-100%The hexane eluent of dichloromethane is purified by column.GD-003 (2.5 g, yield: 60%) was obtained.
According to the analysis of related databases, 1609373-99-0, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Zhejiang Huaxian Optoelectric Technology Co., Ltd.; Zheng Xianzhe; Wang Shichao; Hu Congcong; Wu Xinwei; Zhao Xiaoyu; (158 pag.)CN109810146; (2019); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem