Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 68470-59-7, name is 2-(Bromomethyl)-6-methylpyridine. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 68470-59-7
(2.0 g, 11.35 mmol), potassium carbonate (2.4 g, 17.03 mmol) and Ib (2.2 g, 11.92 mmol) were added to DMF (20 mL), respectively, and stirred overnight at room temperature.The reaction was poured into water and extracted with EtOAc (100 mL x 2).The organic phase was washed with water and saturated brine, and dried over sodium sulfate.After filtration, the filtrate was concentrated and separated by column chromatography (EtOAc / Pet. Ether, 1/10 to 1/4, v / v) to give the product as pale white solid 1c (1.6 g, 50%)
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Reference:
Patent; Suzhou Xiangshi Pharmaceutical Development Co., Ltd; Bu, Xianyong; Yuehan, Fuchuier; Andongni, Kuzubi; Wu, Leguang; Liu, Shiqiang; (30 pag.)CN105985322; (2016); A;,
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