The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 128071-75-0, name is 2-Bromonicotinaldehyde. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 128071-75-0
Wittig Reaction (8) (0263) Ethyl (triphenylphosphoranylidene) acetate (2.80 g, 8.17 mmol) was added to a solution of 2-bromonicotinaldehyde (1.0 g, 5.4 mmol) in dry DCM (dichloromethane) at 0 C. and stirred for 8 h at room temperature. The solvent was then evaporated under vacuum. The colorless oil was partitioned between ethylacetate and water. The organic layer was washed with water, brine and dried over Na2SO4. It was then filtered and evaporated to give an oil from which the title compound 8 was isolated by column chromatography (Si-gel, PE: EA=15:1). Yield: 1.3 g, 94%; State:colorless oil.
With the rapid development of chemical substances, we look forward to future research findings about 128071-75-0.
Reference:
Patent; The Florida State University Research Foundation, Inc.; Alabugin, Igor V.; Mondal, Sayantan; Mohamed, Rana K.; (60 pag.)US2016/347778; (2016); A1;,
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