As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 13362-78-2, name is (E)-1,2-Di(pyridin-4-yl)ethene, molecular formula is C12H10N2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. COA of Formula: C12H10N2
General procedure: Equimolar amounts of 1,10-diiodoperfluorodecane (1e) and dipyridyl 2a or its ethylene analogue 2b were dissolved in a vial containing chloroform at room temperature and in a vial. The open vial was closed in a cylindrical bottle containing paraffin oil. Chloroform was allowed to diffuse at room temperature and after two days 1e·2a,b were isolated as white crystals, washed with n-pentane, and characterized.
With the rapid development of chemical substances, we look forward to future research findings about 13362-78-2.
Reference:
Article; Catalano, Luca; Metrangolo, Pierangelo; Pilati, Tullio; Resnati, Giuseppe; Terraneo, Giancarlo; Ursini, Maurizio; Journal of Fluorine Chemistry; vol. 196; (2017); p. 32 – 36;,
Pyridine – Wikipedia,
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