New downstream synthetic route of 103-74-2

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,103-74-2, its application will become more common.

Adding a certain compound to certain chemical reactions, such as: 103-74-2, 2-(2-Hydroxyethyl)pyridine, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 103-74-2, blongs to pyridine-derivatives compound. Recommanded Product: 103-74-2

To a solution of 2-(2-hydroxyethyl)pyridine (3 ml, 26.6 mmol) was added 30 ml of 33% HBr in acetic acid. The yellow solution was heated in the capped vial at 78 C. for 2 days. The reaction was evaporated under high vacuum to produce a brown solid. The solid was re-crystallized from hot isopropanol to produce a light tan solid (73%). 1H NMR (500 MHz, dMSO): delta 3.62-3.65 (t, 2H), 3.95-3.98 (t, 2H), 7.95 (t, 1H), 8.09-8.10 (d, 1H), 8.58 (t, 1H), 8.90 (d, 1H).

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,103-74-2, its application will become more common.

Reference:
Patent; Tachdjian, Catherine; Lebl-Rinnova, Marketa; Wallace, David; US2006/263411; (2006); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem