Analyzing the synthesis route of 133362-99-9

According to the analysis of related databases, 133362-99-9, the application of this compound in the production field has become more and more popular.

Related Products of 133362-99-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 133362-99-9, name is 2-Pyridin-4-ylbenzoic acid, molecular formula is C12H9NO2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

EXAMPLE 115 2-(4-Pyridinyl)-N-(4-{[2-(2-pyridinyl)ethyl]amino}phenyl)-benzamide The title compound was obtained from tert-butyl 4-aminophenyl[2-(2-pyridinyl)ethyl]carbamate and 2-(4pyridinyl)benzoic acid in the same manner as in Example 101. 1H-NMR (DMSO-d6): delta2.96 (2H, t, J=7.3 Hz), 3.28-3.44 (2H, m), 5.55 (1H, t, J=5.7 Hz), 6.52 (2H, d, J=8.8 Hz), 7.18-7.38 (4H, m), 7.46 (2H, dd, J=1.4 Hz, 10.2 Hz), 7.49-7.68 (4H, m), 7.70 (1H, dt, J=1.8 Hz, 7.6 Hz), 8.51 (1H, d, J=4.1), 8.57 (2H, d, J=6.0 Hz), 9.94 (1H, s) (+)APCI-MS (m/z): 395 (M+H)+

According to the analysis of related databases, 133362-99-9, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Takasugi, Hisashi; Terasawa, Takeshi; Inoue, Yoshikazu; Nakamura, Hideko; Nagayoshi, Akira; Ohtake, Hiroaki; Furukawa, Yoshiro; Mikami, Masafumi; Hinoue, Kazumasa; Ohtsubo, Makoto; US2004/58903; (2004); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem