Related Products of 113124-09-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 113124-09-7, name is 5,6-Dimethylnicotinonitrile. This compound has unique chemical properties. The synthetic route is as follows.
13,0 g of trifluoromethane sulfonic acid was added dropwise to a mixture of 0,91 g (7,0 mmol)2,3-dimethylpyridi ne-5-carbonitrile and 2,0 g (9,0 mmol) I -(2-fluorophenyl)-2-(2-pyridyl)propan-2-olin 40 ml dichloroethane at 0 – 5C. After 2 days at room temperature the reaction mixture was poured onto sodium carbonate solution, the organic layer was separated and the aqueous layer was extracted with dichloromethane. The combined organic extracts were extracted withsodium hydrogen carbonate and water, evaporated and the residue was purified via MPLC with water/acetonitrile mixtures to yield 0,11 g (4 %) of the title compound as a light yellow oil. 1H.NMR (CDCI3, 6 in ppm): 8,7 (s, 1H); 8,6 (d, 1H); 7,8 (m, 2H); 7,6 (m, 1H); 7,3-7,1 (m, 4H);3,4 (d, IH); 3,3, (d, IH); 2,6 (s, 3H); 2,4 (s, 3H); 1,6 (s, 6H).*HPLCMS: Rt = 0,743 mm; M+H = 346,1
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 113124-09-7, 5,6-Dimethylnicotinonitrile.
Reference:
Patent; BASF SE; MUELLER, Bernd; CAMBEIS, Erica; LOHMANN, Jan Klaas; ESCRIBANO CUESTA, Ana; WOLF, Antje; FEHR, Marcus; RIEDIGER, Nadine; TERTERYAN-SEISER, Violeta; GRAMMENOS, Wassilios; WINTER, Christian; (151 pag.)WO2018/54721; (2018); A1;,
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