Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 90395-45-2, name is 1-(4-(Pyridin-3-yl)phenyl)ethanone. A new synthetic method of this compound is introduced below., Recommanded Product: 1-(4-(Pyridin-3-yl)phenyl)ethanone
1-(4-Pyridin-3-ylphenyl)-ethanone (75 g, 380.26 mmole), 3-bromobenzaldehyde (3-bromo) -benzaldehyde) (67g, 362.16mmole), add 1340 ml of ethanol to the reaction flask, and finally add sodium tert-butoxide (52.7 g, 543.23 mmole) at room temperature. After the reaction is complete, add 200 ml. The mixture was filtered with deionized water, and the solid was filtered, washed with deionized water and methanol. The solid was then stirred with 100 ml of deionized water and 200 ml of methanol for 30 minutes. The solid was dried twice to obtain 78 g of pale yellow solid. 3-(3-Bromophenyl)-1-(4-pyridin-3-ylphenyl)-propanone (3-(3-Bromo-phenyl)-1-(4-pyridin-3-yl-phenyl)- Propanone), yield 88.7%
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Reference:
Patent; E-ray Optoelectronics Technology Co Ltd; Huang, Heh Lung; Guo, Huang Ming; Chao, Teng Chih; Lin, Chi Jen; Chang, Min Jong; (53 pag.)TW2019/30287; (2019); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem