A new synthetic route of 18513-79-6

The synthetic route of 18513-79-6 has been constantly updated, and we look forward to future research findings.

Adding a certain compound to certain chemical reactions, such as: 18513-79-6, 1,2,3,6-Tetrahydropyridine hydrochloride, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Computed Properties of C5H10ClN, blongs to pyridine-derivatives compound. Computed Properties of C5H10ClN

The foregoing 3-oxide can also be obtained as follows: 40 g. of 1,2,5,6-tetrahydropyridine hydrochloride and 30 g. of sodium dicyanamide are suspended in 400 ml. of n-butanol and 30 ml. of water and heated to reflux overnight. The mixture is cooled and filtered and the filtrate is evaporated. The residue is digested in 100 ml. of water and the solid substance is filtered off and recrystallized from o-xylene, there being obtained pure 1-(1,2,5,6-tetrahydropyridine)-3-cyanoguanidine having a melting point of 131-133 C.

The synthetic route of 18513-79-6 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; Hoffmann-La Roche Inc.; US4276417; (1981); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem