Quality Control of Phenyl(pyridin-2-yl)methanone. Recently I am researching about ONE-POT SYNTHESIS; ARYL HALIDES; DERIVATIVES; ALCOHOLS; FLUORIDE; MECHANOCHEMISTRY; NANOPARTICLES; HYDROCARBONS; ACTIVATION; VINYLATION, Saw an article supported by the US Department of Energy, Office of Science, Basic Energy Sciences, Materials Sciences and Engineering DivisionUnited States Department of Energy (DOE) [DE-AC02-76SF00515]. Published in WILEY-V C H VERLAG GMBH in WEINHEIM ,Authors: Hosseini, A; Schreiner, PR. The CAS is 91-02-1. Through research, I have a further understanding and discovery of Phenyl(pyridin-2-yl)methanone
Ball milling of calcium carbide (CaC2) enables the reaction of its ethynyl moiety with organic electrophiles. This was realized simply by co-milling CaC(2)with organic substrates in a sealed jar without the need for an additive or a catalyst. Various ketones including those bearing alpha-hydrogens were ethynylated in good yields at short reaction times. Aryl halides are also amenable substrates for this protocol as they furnish aryl ethynes through a benzyne intermediate. This method offers a practical and cheap alternative to the established procedures for introducing ethynyl functionalities.
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Reference:
Pyridine – Wikipedia,
,Pyridine | C5H5N – PubChem