Analyzing the synthesis route of (4,6-Dichloropyridin-3-yl)methanol

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 73998-95-5, (4,6-Dichloropyridin-3-yl)methanol, other downstream synthetic routes, hurry up and to see.

Application of 73998-95-5, Adding some certain compound to certain chemical reactions, such as: 73998-95-5, name is (4,6-Dichloropyridin-3-yl)methanol,molecular formula is C6H5Cl2NO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 73998-95-5.

(b) 5-Chloromethyl-2,4-dichloropyridine 20.2 g. of 2,4-dichloropyridin-5-methanol (0.11 mol.) and 150 ml. of phosphorus oxychloride are refluxed for 19 hours. Then the excess phosphorus oxychloride is removed in vacuo and ice is added to the residue. 5-Chloromethyl-2,4-dichloropyridine is filtered off, washed with water, dried in the desiccator over P2 O5 and recrystallized from hexane; yield 17.95 g. (83%), m.p. 55-56.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 73998-95-5, (4,6-Dichloropyridin-3-yl)methanol, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; E. R. Squibb & Sons, Inc.; US4191831; (1980); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem