Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 935466-69-6, name is 4-Chloro-1H-pyrrolo[2,3-b]pyridin-6-amine. A new synthetic method of this compound is introduced below., Product Details of 935466-69-6
The compound (11.0g, 65.6mmol) obtained in Step 2 was dissolved in pyridine (100ml) and cyclopropanecarbonyl chloride (7.5g, 72.2mmol) was slowly added dropwise at 0oC, followed by stirring at the same temperature for 1 hour. The reaction mixture was added to water (350 ml), and the resulting solid was filtered and dried under reduced pressure to obtain the title compound (12.7 g, 53.9 mmol)
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Reference:
Patent; H Kei Ino N Co., Ltd.; Ryu Ha-na; Kim Dong-gyu; Jeong Su-yeon; Ji Mi-gyeong; Lee Hyeok-u; Kim Seung-chan; Ki So-yeong; Kim Myeong-jung; Lee Ye-rim; Lee Ho-yeol; Park Ji-yeon; (334 pag.)KR102112336; (2020); B1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem