Beccalli, Egle M.; Broggini, Gianluigi; Paladino, Giuseppe; Zoni, Caterina published an article in Tetrahedron. The title of the article was ãPalladium-mediated approach to dibenzo[b,e][1,4]diazepines and benzopyrido-analogues. An efficient synthesis of tarpaneã?Recommanded Product: 1028-86-0 The author mentioned the following in the article:
An original synthetic route toward dibenzo[b,e][1,4]diazepin-11-ones, e.g., I, and analogs pyridobenzodiazepinones has been developed. The method relied upon an intramol. amination process between an (hetero)aryl halide and the appropriate aniline moiety. In the experimental materials used by the author, we found N-(2-Chloropyridin-3-yl)-2-nitrobenzamide(cas: 1028-86-0Recommanded Product: 1028-86-0)
N-(2-Chloropyridin-3-yl)-2-nitrobenzamide(cas: 1028-86-0) belongs to anime. To avoid the problem of multiple alkylation, methods have been devised for âblockingâ?substitution so that only one alkyl group is introduced. The Gabriel synthesis is one such method; it utilizes phthalimide, C6H4(CO)2NH, whose one acidic hydrogen atom has been removed upon the addition of a base such as KOH to form a salt.Recommanded Product: 1028-86-0