Synthetic Route of 1137-67-3, Adding some certain compound to certain chemical reactions, such as: 1137-67-3, name is 2-(Pyridin-3-yl)-1H-benzo[d]imidazole,molecular formula is C12H9N3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1137-67-3.
Complex 1 waspreparedbylayeringmethod.Abufferlayerof asolution(10ml)ofacetonitrile-water(1:1,v/v)wascarefullylayeredover5mlofanaqueoussolutionof alpha-H3PMo12O40 6H2O(120mg,0.06mmol).Thenamethanol(5ml)of3-PyBim(23.4 mg,0.12mmol)wascarefullylayeredoverthebufferlayer.Tendayslater,redcrystalsappearedandwerecollectedanddriedin airafterquicklybeingwashedwithwater.Yield:108mg,91%based on alpha-H3PMo12O40 6H2O. Anal.Calcd(%)forC27H35Mo12-N7O44.5P: C,13.79;H,1.50;N,4.17;Found(%):C,13.71;H,1.42;N,4.08. IR(KBr) nu, cm1: fourcharacteristicvibrationsresultingfromheteropolyanionswiththeKegginstructure:803 nu(Mo-Oc), 878 nu(Mo-Ob), 961 nu(MoOt), 1065 nu(P-Oa); (Ot, terminal oxygenatomsconnecting oneMoatom;Ob, atomslocatedinasharedcornerbetweentwoMo 3O13 units; Oc, oxygenatomsconnectingedge-sharing MoO6 octahedra inaMo3O13 unit); andanothervibrationsresulting from3-PyBimmolecules:1449,1402,1316and1118
According to the analysis of related databases, 1137-67-3, the application of this compound in the production field has become more and more popular.
Reference:
Article; Wei, Mei-Lin; Wang, Yu-Xia; Wang, Xin-Jun; Journal of Solid State Chemistry; vol. 209; (2014); p. 29 – 36;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem