Category: 1008-91-9

Adding a certain compound to certain chemical reactions, such as: 1008-91-9, 1-(Pyridin-4-yl)piperazine, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, SDS of cas: 1008-91-9, blongs to pyridine-derivatives compound. SDS of cas: 1008-91-9

General procedure: A mixture of compound 4-6 (1 mmol) in 5 ml of dry DCM and piperazine derivative (1 mmol) was cooled in an ice bath. Then, 1.1 mmol of DCC in 5 ml of dry dichloromethane was added to the mixture under nitrogen (N2) atmosphere. Reaction mixture was stirred for 0.5 hour in an ice bath, then 10-16 hours at room temperature. Reaction solvent was evaporated to the dryness. Residue was dissolved in hot acetonitrile then cooled in refrigerator to get the DCU precipitated. White crystalline DCU was removed by filtration. Liquid part was evaporated and crystallized from appropriate solvents to give compound 7-34

The synthetic route of 1008-91-9 has been constantly updated, and we look forward to future research findings.

Reference:
Article; Akgun, Hulya; Yilmaz, Demet Us; Atalay, Rengul Cetin; Gozen, Damla; Letters in drug design and discovery; vol. 13; 1; (2016); p. 64 – 76;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem

1008-91-9, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1008-91-9, name is 1-(Pyridin-4-yl)piperazine. This compound has unique chemical properties. The synthetic route is as follows.

A mixture ofCu(NO3)23H2O (0.2 mmol, 48 mg), 1-(pyridin-4-yl)piperazine(0.2 mmol, 33 mg) and Na2C2O4 (0.4 mmol, 54 mg) inwater (2 ml), dimethylformamide (DMF, 2 ml) and methanol(2 ml) was adjusted to pH 2 by adding 0.1 M HNO3 and stirringwas carried out for 5 min. The mixture was then sealed ina 20 ml glass vial, heated at 373 K for 1 d and cooled slowly toroom temperature. Blue crystals of (I) were obtained in a yieldof 14% (11 mg, based on the copper salt). Elemental analysiscalculated for CuC13H15N3O8: C 38.57, H 3.73, N 10.38%;found: C 38.22, H 3.56, N 10.65%. FT-IR peaks (ATR cell, ,cm1): (NH) 2755 (br); (C N) 1670 (m); as(OCO) 1617(s), 1516 (m); s(CO) 1407 (m); s(CO)+(OCO) 1287 (s), 1219(w), 1144 (w), 1027 (w), 923 (w); (OCO) 790 (s). UV-Vis(diffuse reflectance, cm1): 14310.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 1008-91-9, 1-(Pyridin-4-yl)piperazine.

Reference:
Article; Klongdee, Fatima; Boonmak, Jaursup; Youngme, Sujittra; Acta Crystallographica Section C: Structural Chemistry; vol. 74; 3; (2018); p. 300 – 306;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem