Application of 13508-96-8, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 13508-96-8, name is 2-Methyl-4-nitropyridine. This compound has unique chemical properties. The synthetic route is as follows.
2-methyl-4-nitropyridine (13.8 g, 0.1 mol) was dissolved in a methanol solution.10% Pd/C (0.1 g) was added, and the reaction was carried out in an autoclave, and hydrogen gas was passed to a pressure of 0.5 MPa, and the temperature was raised to 30 C for 15 hours.TLC was monitored until the reaction was complete, cooled to room temperature, diatomaceous earth was filtered, and the filter cake was washed with dichloromethane.This prevents Pd/C from catching fire and the filtrate is concentrated to give 2-methyl-4-aminopyridine.The molar yield was 97%.
According to the analysis of related databases, 13508-96-8, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Danyang Ning David Fang To Detect Co., Ltd.; Wei Qian; (5 pag.)CN109748854; (2019); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem