Authors Chen, YJ; Xiang, Y; He, YH; Guan, Z in PERGAMON-ELSEVIER SCIENCE LTD published article about CARBON BOND FORMATION; ONE-POT SYNTHESIS; SILOXY SERINE ORGANOCATALYST; DYNAMIC KINETIC RESOLUTION; DIELS-ALDER REACTION; BETA-AMINO; BIOCATALYTIC PROMISCUITY; ENANTIOSELECTIVE SYNTHESIS; ENZYME PROMISCUITY; ALPHA-CHYMOTRYPSIN in [Chen, Yu-Jue; Xiang, Yang; He, Yan-Hong; Guan, Zhi] Southwest Univ, Sch Chem & Chem Engn, Key Lab Appl Chem Chongqing Municipal, Chongqing 400715, Peoples R China in 2019.0, Cited 69.0. Safety of 3-Pyridinecarboxaldehyde. The Name is 3-Pyridinecarboxaldehyde. Through research, I have a further understanding and discovery of 500-22-1
The anti-selective direct asymmetric Mannich reaction of (hetero) aromatic aldehydes, 4-anisidine and O-protected hydroxyacetones for the synthesis of stereodefined anti-beta-amino-alpha-hydroxycarbonyl compounds was developed. Protease type XIV from Streptomyces griseus (SGP) was used as a biocatalyst in 1,4-dioxane/phosphate buffer under mild reaction conditions. The excellent diastereoselectivities of up to >99:1 (anti/syn) and good enantioselectivities of up to 90% ee were achieved. This method provides a more sustainable complement to chemically catalyzed anti-selective direct asymmetric Mannich reactions. (C) 2019 Elsevier Ltd. All rights reserved.
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Reference:
Pyridine – Wikipedia,
,Pyridine | C5H5N – PubChem