Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 945954-95-0, name is 6-Bromo-3-methoxypicolinaldehyde. This compound has unique chemical properties. The synthetic route is as follows. COA of Formula: C7H6BrNO2
To a solution of 6-bromo-3-methoxypicolinaldehyde (0.13 g, 0.60 mmol) in THF (6 mL) and tBuOH (6 mL) was added 2-methyl-2-butene (0.64 mL, 2.41 mmol), followed by an aqueous solution (2 mL) of sodium dihydrogen phosphate (0.29 mg, 2.4 mmol) and NaC102 (0.22 mg, 2.4 mol). The resulting mixture was stirred at RT for 16 hrs. The volatiles were then evaporated in vacuo and the residue thus obtained was purified on silica gel eluting with a solvent gradient of 0 to 10% MeOH in DCM (with 2% acetic acid as an additive in DCM) to afford 6-bromo-3-methoxypicolinic acid as a solid.
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 945954-95-0, 6-Bromo-3-methoxypicolinaldehyde.
Reference:
Patent; INCEPTION 2, INC.; STOCK, Nicholas, Simon; CHEN, Austin, Chih-Yu; BRAVO, Yalda, Mostofi; JACINTHO, Jason, Duarte; SCOTT, Jill, Melissa; STEARNS, Brian, Andrew; CLARK, Ryan, Christopher; TRUONG, Yen, Pham; WO2013/134562; (2013); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem