Synthetic Route of 91182-50-2, Adding some certain compound to certain chemical reactions, such as: 91182-50-2, name is 3-Bromo-2-phenylpyridine,molecular formula is C11H8BrN, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 91182-50-2.
Molecules 1 (2 mmol, 466 mg) and iridium trichloride trihydrate (1 mmol, 352 mg) were weighed into a round-bottomed flask, evacuated, and bubbling nitrogen, and circulated three times. Under a nitrogen atmosphere, 16 mL of a mixed solution of ethylene glycol ether and water (3: 1, v / v) was injected and dissolved by stirring. After reacting at 110 C for 24 hours, the crude product was cooled to room temperature, and filtered through a sand core funnel to obtain a solid, which was washed three times with deionized water and ethanol. The product is obtained after drying in a vacuum drying box.
According to the analysis of related databases, 91182-50-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Nanjing University of Posts and Telecommunications; Zhang Yin; Wang Jun; Lan Yiping; Zhao Qiang; Liu Shujuan; Huang Wei; (11 pag.)CN110330532; (2019); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem