1003-68-5, Adding a certain compound to certain chemical reactions, such as: 1003-68-5, 5-Methylpyridin-2(1H)-one, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 1003-68-5, blongs to pyridine-derivatives compound.
A single-necked flask was charged with 0.1 g (1 mmol) of 5-methyl-2 (1H)one 0.14 g K2CO3, 0.17 g p-bromobenzaldehyde,0.05 g CuI, 5 ml DMF as solvent,The reflux reaction was carried out,TCL monitoring to the reaction is completed,Stop reaction, filter,The filtrate was extracted with EA (ethyl acetate)The organic layer was concentrated (PE: EA = 3: 1, volume ratio, PE was petroleum ether)To give a yellowish or white flake solid 0.08 g,That is compound 1.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,1003-68-5, its application will become more common.
Reference:
Patent; Sichuan University; Yin, Shufan; Li, Yong; Cao, Tingting; Yuan, Li; Song, Zhangwei; (16 pag.)CN106397408; (2017); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem