Electric Literature of 18820-82-1, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 18820-82-1, name is Pyridine hydrobromide. A new synthetic method of this compound is introduced below.
A 5 mL water solution of NiCl2*6H2O (0.5950 g, 2.50 mM) was added into 10 mL methanol solution of Na2tdas (0.9710 g, 5.00 mM), and the solution was stirred for one hour. The solution above was then added into 10 mL water solution of N-hydrogenpyridinium bromide (0.8000 g, 5.00 mM), and the mixture was stirred for ten minutes, during which a brownish sediment appeared. Brownish microcrystals were obtained after recrystallization of the brownish sediment from diethyl ether.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,18820-82-1, Pyridine hydrobromide, and friends who are interested can also refer to it.
Reference:
Article; Wang, Chi-Feng; Qiao, Fang; Chi, Yan-Hui; Shi, Jing-Min; Cottrill, Ethan; Pan, Ning; Zhu-Ge, Wei-Wei; Fu, Yong-Xin; Xu, Jun; Qian, Xiao-Ping; Journal of Coordination Chemistry; vol. 68; 21; (2015); p. 3884 – 3893;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem