Application of 13362-78-2, In the chemical reaction process,reaction time,type of solvent,can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product.An updated downstream synthesis route of 13362-78-2 as follows.
A mixture of ZnSO4* 7H2O (0.05mmol, 0.010g), H2L (0.025mmol ,0.006g), DPE (0.025mmol 0.005g), NaOH (0.025mmol,0.001g) and H2O (8mL) was sealed in a Teflon-lined autoclave and heated at 120 °C for 3 days,then followed by slow cooling to room temperature. The yield of the colorless block crystals is ca.68percent based on H2L. Elemental Anal. Found:C, 55.8;H,3.5;N,8.1percent. Calcd. for ZnC25H21N3O7: C,55.5;H,3.9;N,7.8percent. IR(cm1) (seeFig.S1): 3325(s),3061(m),1637(s),1568(s),1418(m),1387(s),1336(m),1281(m),1194(s),1148(w),1037(m),1017(m),964(m),842(s),769(m),671(m),549(s),462(m).
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,13362-78-2, its application will become more common.
Reference:
Article; Yan, Xingxiu; Qiu, Xiandeng; Yan, Zhishuo; Li, Hongjiang; Gong, Yun; Lin, Jianhua; Journal of Solid State Chemistry; vol. 237; (2016); p. 313 – 322;,
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