Application of 115473-15-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 115473-15-9, name is 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridin-2(4H)-one hydrochloride, molecular formula is C7H10ClNOS, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Example-5: Purification of 5,6,7,7a-tetrahydro-4H-thieno[3,2-c]-pyridin-2-one- hydrochloride A mixture of dichloromethane (425 ml), methanol (75 ml) and 5,6,7,7a-tetrahydro-4H- thieno[3,2-c]-pyridin-2-one-hydrochloride (100 grams) was heated to reflux. The reaction mixture was stirred for 30 minutes and cooled to 25-30C and further stirred for 1 hour. The solid obtained was filtered, washed with dichloromethane and dried to get the title compound.Yield: 88 grams; Assay: 98.5%
According to the analysis of related databases, 115473-15-9, the application of this compound in the production field has become more and more popular.
Reference:
Patent; MSN LABORATORIES LIMITED; SATYANARAYANA REDDY, Manne; THIRUMALAI RAJAN, Srinivasan; ELEVATHINGAL NICHOLAS, Madhu; RAMA SUBBA REDDY, Karamala; WO2011/92720; (2011); A2;,
Pyridine – Wikipedia,
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