Application of 120739-77-7, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 120739-77-7, name is N-((6-Chloropyridin-3-yl)methyl)ethanamine, molecular formula is C8H11ClN2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
2): Synthesis of N-(6-chloropyridin-3-yl)methylene)-N-ethyl-1-(methylthio)-2-nitrovinylidene amine To a 100 ml three necked round bottom flask, N-(6-chloropyridin-3-yl-methylene)ethylamine (17.0 g, 0.1 mol), 1,1-bis(methylthio)-2-nitroethene (15.0 g, 0.09 mol), anhydrous ethanol (50 mL) were added. The mixture was refluxed until full convention and cooled to r.t., The reaction was concentrated with reduced pressure to obtain a crude product as dense liquid, which was purified by column chromatography to yield 5.3 g N-(6-chloropyridin-3-yl-methylene)-N-ethyl-1-(methylthio)-2-nitrovinylidene amine in 18.5% yield.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 120739-77-7, N-((6-Chloropyridin-3-yl)methyl)ethanamine.
Reference:
Patent; EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY; US2010/298346; (2010); A1;,
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