Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 92914-74-4, name is Isoxazolo[5,4-b]pyridin-3-amine. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 92914-74-4
General procedure: To a solution of 3-aminoisoxazolo[5,4-b]pyridine(1) (1.35 g, 0.01 mol) in tetrahydrofurane (100mL) a few drops of pyridine and benzoyl chloride or4-bromobenzoyl chloride or 4-chlorobenzoyl chloridewas added. The reaction mixture was heatedunder reflux while being stirred in the microwavereactor in an aluminum bath at 60-65OC for 15 min.(3 5 min. with 5 min. breaks) at microwave powerP = 240 W. The solvent was removed under reducedpressure. The residue obtained was triturated withwater, filtered, dried and crystallized from ethanol.
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Reference:
Article; Por?ba, Krystyna; Pawlik, Krzysztof; Rembacz, Krzysztof P.; Kurowska, Ewa; Matuszyk, Janusz; D?ugosz, Anna; Acta poloniae pharmaceutica; vol. 72; 4; (2015); p. 727 – 735;,
Pyridine – Wikipedia,
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