Reference of 63071-03-4, Adding some certain compound to certain chemical reactions, such as: 63071-03-4, name is 2-Methoxy-6-methylpyridine,molecular formula is C7H9NO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 63071-03-4.
To intermediate 73 (1.95 g, 0.015 mol) at r. t. , was added HNO3 60% (7ml). The mixture became reddish brown with generation of heat and NO2. CONC. H2SO4 (7ML) was then added. The solution was stirred at 80C overnight. Into the cooled reaction mixture was poured ice water (70ml) and the solution was neutralized with CACO3. The aqueous solution was extracted with EtOAc (3X50 mL) and the combined organic extracts were dried over anh. NA2SO4. The solids were filtered and the solvent was evaporated to dryness to give the title compound (2.25 g, 86%) as a yellow solid. NMR (‘H, DMSO): 8 8.3 (d, 1H) ; 6.8 (d, 1H) ; 4 (s, 3H), 2.7 (s, 3H).
According to the analysis of related databases, 63071-03-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; SB PHARMCO PUERTO RICO INC; NEUROCRINE BIOSCIENCES INC; GLAXO GROUP LIMITED; WO2004/62665; (2004); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem