Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 56673-34-8, name is 3-Bromo-6-mercaptopyridine. This compound has unique chemical properties. The synthetic route is as follows. name: 3-Bromo-6-mercaptopyridine
General procedure: To a mixture of thiol (0.35mmol) in iPrOH in a 10mL vial, Rose Bengal (0.05equiv) were added and the reaction mixture was stirred at room temperature under white LED irradiation. The reaction mixture was quenched by addition of saturated aqueous NaOH (10mL), extracted with Et2O (3×10mL), dried over Na2SO4 and evaporated under reduced pressure to give the desired product.
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Reference:
Article; Tankam, Theeranon; Poochampa, Kamolrut; Vilaivan, Tirayut; Sukwattanasinitt, Mongkol; Wacharasindhu, Sumrit; Tetrahedron; vol. 72; 6; (2016); p. 788 – 793;,
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