In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 94446-97-6, name is 2-Bromo-3-(bromomethyl)pyridine, the common compound, a new synthetic route is introduced below. Recommanded Product: 94446-97-6
Step 2: To a solution of the product of Step 1 (595 mg, 2.36 mmol) in DMF was added piperidine (205 mg, 2.4 mmol) and K2CO3 (979 mg, 7.08 mmol), sequentially. The mixture was stirred at rt overnight, quenched with ice-water and then partitioned with ether. The organic layer was dried over Na2SO4, filtered, and concentrated. Purification of the residue by SiO2 chromatography (0-50% EtOAc/hexane) gave the desired compound (-450 mg). CnH15BrN2, LC/ESI-MS: m/z 255 and 257 (C11H15BrN2 H+)
The synthetic route of 94446-97-6 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; SCHERING CORPORATION; WO2007/53435; (2007); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem