Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 1195-59-1, name is 2,6-Pyridinedimethanol. A new synthetic method of this compound is introduced below., Recommanded Product: 1195-59-1
The 2,6-dimethylolpyridine (10.0g, 71. 9mmol) by adding 250 ml three flasks, constant voltage used in the dropping funnel slowly dropping 48% of HBr (95 ml) solution dissolved, after maintaining the 60 C magnetic stirring for 19 hours. After the end of the reaction cooled to the room temperature, and then to continue to use the ice ice salt bath cooling and saturation of the sodium accent carbonate to alkaline. The generated white solid after filtering, washing several times with distilled water, then the n-hexane recrystallization under the room temperature condition, to obtain the colorless transparent acicular crystal (12.3g, 65%). Mass spectrum: ES – MS (CH3CN), m/z (%): 266.00 (100) [M + H]+. 2. 6 – dibromo methyl pyridine (B) in acetonitrile electrospray mass spectrum chart of Figure 1.
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 1195-59-1, 2,6-Pyridinedimethanol.
Reference:
Patent; Nanjing University; WANG, ZHILIN; GENG, ZHIRONG; (25 pag.)CN106518896; (2017); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem