Adding a certain compound to certain chemical reactions, such as: 350-03-8, 1-(Pyridin-3-yl)ethanone, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, name: 1-(Pyridin-3-yl)ethanone, blongs to pyridine-derivatives compound. name: 1-(Pyridin-3-yl)ethanone
A mixture of 30 g of 3-acetylpyridine and 60 g of N, -dimethylformamidedimethylacetal was stirred for 6 hours under reflux with heat. After cooling down to room temperature, the mixture was concentrated under reduced pressure. 3-dimethylamino-l- (pyridin-3-yl ) – propenone (43 g) was obtained. 1 H-N R (CDC13) delta: 9.09-9.07 (1H, m) , 8.68-8.65 (1H, m) , 8.19 (1H, dt), 7.85 (1H, d) , 7.38-7.34 (1H, m) , 5.68 (1H, d) , 3.19 (3H, s), 2.96 (3H, s).
At the same time, in my other blogs, there are other synthetic methods of this type of compound,350-03-8, 1-(Pyridin-3-yl)ethanone, and friends who are interested can also refer to it.
Reference:
Patent; SUMITOMO CHEMICAL COMPANY, LIMITED; ARIMORI, Sadayuki; SHUTO, Akira; MIZUNO, Hajime; WO2011/49150; (2011); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem