Application of 59576-31-7, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 59576-31-7, name is 1-(4,6-Dimethylpyridin-2-yl)ethanone, molecular formula is C9H11NO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Example 7: Preparation of compound P.10l-(4,6-Dimethyl-pyridin-2-yl)-ethanone (400mg) was dissolved in methanol (15ml_) and (E)-l-[6-(3-aminooxy-propyl)-pyridin-2-yl]-ethanone O-methyl-oxime (600mg) was added. After stirring for 70h at ambient temperature, the reaction mixture was concentrated and the residue was purified by chromatography over silica to give colorless oil (740mg). ^-NMR (CDCI3, 400 MHz):7.70 (d, IH), 7.55 (t, IH), 7.47 (s, 2H), 7.11 (d, IH), 6.93 (s, IH), 4.28 (t, 2H), 4.01 (s, 3H), 2.92 (t, 2H), 2.51 (s, 3H), 2.32 (s+s+s, 9H), 2.21 (m, 2H)
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 59576-31-7, 1-(4,6-Dimethylpyridin-2-yl)ethanone.
Reference:
Patent; SYNGENTA PARTICIPATIONS AG; ZAMBACH, Werner; STIERLI, Daniel; NEBEL, Kurt; BORTOLATO, Andrea; MASSOL-FRIEH, Clara; WO2012/38521; (2012); A1;,
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