Application of 60753-14-2 ,Some common heterocyclic compound, 60753-14-2, molecular formula is C9H13NO, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
7.561 g (0.05 mol) of 4-(3-pyridyl)-1-butanol and 19.020 g (0.05 mol) of 1-iodooctadecane were added to a three-necked flask.Add 70 ml of N,N-dimethylformamide,Then at 120 C,Stir the reaction for 12 hours,Cool to room temperature,After the reaction is over,Purifying the reaction product,After completely removing the monomer not involved in the reaction,Vacuum drying to constant weight,getIodinated 1-octadecyl-3-pyridinium butanol quaternary ammonium salt.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 60753-14-2, 4-(Pyridin-3-yl)butan-1-ol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; South China University of Technology; Liu Fang; He Jingwei; Zhang Yunlong; (13 pag.)CN108484487; (2018); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem