Related Products of 76469-41-5 ,Some common heterocyclic compound, 76469-41-5, molecular formula is C5H2F3N, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
6.65 g of the compound obtained in Step 3 and 4.6 ml of hydrazine monohydrate were added to 100 ml of n-propanol. The resulting mixture was refluxed for 6 hours, and distilled under a reduced pressure to remove the solvent. The residue thus obtained was dissolved in 80 ml of chloromethane, washed with water, and dried over anhydrous magnesium sulfate. The resulting organic layer was concentrated under a reduced pressure to obtain 6.20 g (yield: 85.6%) of the title compound.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 76469-41-5, 2,3,5-Trifluoropyridine, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Park, Tae-Ho; Zhao, Long-Xuan; Lee, Sang-Ho; US2006/47124; (2006); A1;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem